Synthesis of inorganic-organic polymers
EURO CERAMICS VIII, PTS 1-3, cilt.264-268, ss.423-426, 2004 (SCI-Expanded)
- Yayın Türü: Makale / Tam Makale
- Cilt numarası: 264-268
- Basım Tarihi: 2004
- Doi Numarası: 10.4028/www.scientific.net/kem.264-268.423
- Dergi Adı: EURO CERAMICS VIII, PTS 1-3
- Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
- Sayfa Sayıları: ss.423-426
- Anahtar Kelimeler: sol-gel method, hybrid nanocomposite material, TGA
- Akdeniz Üniversitesi Adresli: Hayır
Özet
In this study, 3-Glycidoxypropyl trimethoxysilane (GLYMO), Methyl triethoxy silane (MTEOS) were hydrolyzed and then polymerized with Aluminium-sec-butoxide, Al(OBus)(3) that is complexed with Ethyl acetoacetate (HacacOEt). The complexation of Aluminium-sec-butoxide with Ethyl acetoacetate was investigated with Fourier Transform Infared Spectroscopy (FT-IR). The storage stability of the obtained sot was determined with viscosity measurements. Thermal behaviour of the hybrid gel was analysed with Thermogravimetric analysis (TGA). The TGA results showed that about 40% of the obtained hybrid polymer is inorganic and 60% is organic.