Study of filling material of dental composites: an analytical approach using radio-activation


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Eke C., Er K., Segebade C., Boztosun İ.

RADIOCHIMICA ACTA, cilt.106, sa.1, ss.69-77, 2018 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 106 Sayı: 1
  • Basım Tarihi: 2018
  • Doi Numarası: 10.1515/ract-2017-2766
  • Dergi Adı: RADIOCHIMICA ACTA
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.69-77
  • Anahtar Kelimeler: Photoactivation analysis (PAA), dental composites, bremsstrahlung photons, semiconductor spectrometry, X-ray fluorescence spectrometry (EDXRF), RAY-FLUORESCENCE ANALYSIS, PHOTON, ACCELERATOR, ELEMENTS, XRF
  • Akdeniz Üniversitesi Adresli: Evet

Özet

The aim of this study is to carry out elemental analyses of dental composites acquired from different producers using photoactivation analysis (PAA). High energy electrons produced by an electron linear accelerator are absorbed by a tungsten disk (Bremsstrahlung converter) thereby producing high energy X-rays (bremsstrahlung). The dental composite materials under study were exposed to the bremsstrahlung radiation whereby radionuclides were produced through photonuclear reactions. Their radioactivities were measured using high resolution semiconductor spectrometers equipped with high purity germanium detectors (HPGe). The spectra were analysed using appropriate computer software. As a result, photonuclear reactions of 12 stable elements were detected in different dental composite species, and the elemental concentrations were calculated. For comparison, the dental composites were also investigated using scanning electron microscopy (SEM) and energy-dispersive X-ray fluorescence spectrometry (EDXRF). Various sizes and shapes of dental composites were observed using SEM. However, contents of dental composites, e.g. Mg, Ni, Ba and Sr were obtained by PAA whilst C, O, Al, S, Ba and Sr were detected by EDXRF spectrometry. The results for Ba and Sr obtained using the two techniques show considerable difference.